VINYL ACETATE: METHOD 1453, Issue 3, dated 15 March 2013 - Page 4 of 4
samples stored for 30 days at 5 °C were 90 to 110% for samples spiked at 187 and 747 µg per sample. The pooled coefficient of variation obtained from replicate determinations of analytical standards in this range was 0.020. [3,9] REFERENCES: [1] EU SCOEL (European union scientific committee on occupational exposure limits for vinyl acetate) [2005]. Recommendation from the scientific committee on occupational exposure limits for vinyl acetate. [1] October 2005. [2] ACGIH [2012]. Documentation of the TLVs® and BEIs® with other worldwide occupational exposure values. Cincinnati, OH: American Conference of Governmental Industrial Hygienists. CD-ROM, ISBN: 978-1-607260-48-6. [3] NIOSH [2013]. Backup data report for vinyl acetate. Cincinnati, OH: US Department of Health and Human Services, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health (unpublished, available on request.) [4] NIOSH [1994]. Vinyl acetate: method 1453. In: Eller PM, Cassinelli ME, eds. NIOSH Manual of Analytical Methods, 4th ed., Cincinnati, OH: US Department of Health and Human Services, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health. Publication No. 94-113. [www.cdc.gov/niosh/docs/2003-154/pdfs/1453.pdf ]. [5] OSHA [1985]. Vinyl acetate: organic method 0051. Salt Lake City, Utah: U.S. Department of Labor, Occupational Safety and Health Administration. [http://www.osha.gov/dts/sltc/methods/organic/ org051/org051.html]. Data accessed October 2012. [6] NIOSH [1978]. Vinyl acetate: P & CAM 278. In: Taylor DG, ed. NIOSH Manual of Analytical Methods, 2nd ed., Vol 4. Cincinnati, OH: U.S. Department of Health, Education, and Welfare, Center for Disease Control, National Institute for Occupational Safety and Health, DHEW (NIOSH) Publication no. 78-175. [7] NIOSH [2005]. NIOSH pocket guide to chemical hazards. Barsan ME, ed. Cincinnati OH: U.S. Department of Health and Human Services, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health. DHHS (NIOSH) Publication no. 2005-149. [8] OSHA [1999]. OSHA occupational safety and health guidelines for vinyl acetate. Salt Lake City, UT: U.S. Department of Labor, Occupational Safety and Health Administration. [http://www.osha.gov/ SLTC/healthguidelines/vinylacetate/recognition.html]. Data accessed on February 6, 2013. [9] Yoon YH, Perkins JB [1998]. Vinyl acetate by GC-FID sample analysis backup data report Salt Lake City, UT: DataChem Laboratories. Developed under contract No. CDC-200-2001-08000 (Unpublished, available on request.) METHOD REVISED BY: 3rd Issue (2013) Y. T. Gagnon and P. F. O’Connor, CDC/NIOSH, Cincinnati, Ohio. 2nd Issue (1998) Y. H. Yoon, Ph.D. and J. B. Perkins, DataChem Laboratories, Inc., Salt Lake City, Utah. 1st Issue (1994) A. A. Grote, CDC/NIOSH, Cincinnati, Ohio.
NIOSH Manual of Analytical Methods (NMAM), Fifth Edition
