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ORGANIC AND INORGANIC GASES by FTIR Spectrometry: METHOD 3800, Issue 1, dated 15 March 2003 - Page 47 of 47



Table E7. Final LSF Results for Final Synthetic Sample Spectra Containing TFE, DFE, Water, and HFP
Synthetic Sample Spectrum File Name TFE Synth. Conc. (ppm) TFE LSF Result (ppm) TFE LSF 3σ Uncert. (%) DFE Synth. Conc. (ppm ) DFE LSF Result (ppm ) DFE LSF 3σ Uncert. (%) H2O LSF Result (arb) H2O LSF 3σ Uncert. (%)
S0011.spc 0 1.00 39.6 0 -1.58 26.5 1.65 0.89
S0022.spc 0 2.01 39.5 0 -3.16 26.4 3.29 1.78
S5511.spc 25.0 24.43 0.27 25.0 24.27 0.33 0.87 12.1
S5112.spc 25.0 24.45 0.27 5.00 4.81 1.72 0.88 12.34
S1511.spc 5.00 4.91 0.44 25.0 24.27 0.11 1.08 3.23
S5522.spc 25.0 24.46 0.28 25.0 24.27 0.35 1.99 5.51
S5121.spc 25.0 24.45 0.27 5.00 4.92 1.63 1.99 5.25
S1522.spc 5.00 4.94 0.57 25.0 24.29 0.14 2.20 2.05
Average Abs. % Concentration Uncertainty[1]     0.35     0.71 6.74
  1. The average excludes the spectra (S0011 and S0022) with zero synthetic TFE and DFE concentrations.

NIOSH Manual of Analytical Methods, Fourth Edition