POLYCHLOROBIPHENYLS: METHOD 5503, Issue 2, dated 15 August 1994 - Page 4 of 5 REFERENCES: [1] [2] [3] [4] [5] [6] [7] [8] [9] [10] [11] [12]
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[15]
NIOSH Manual of Analytical Methods, 2nd ed., V. 1, P&CAM 244, U.S. Department of health, Education, and Welfare, Publ. (NIOSH) 77-157-A (1977). User check, Southern Research Institute, NIOSH Sequence #4121-U (unpublished, January 25, 1984). Kominsky, J. Applied Ind. Hyg. 1 (4), R-6 (1986). NIOSH Health Hazard Evaluation Report, HETA 85-289-1738 (unpublished, 1986). Hofstader, R. A., C. A. Bache, and D. J. Lisk. Bull, Environ. Contam. Toxicol., 11, 136 (1974). NIOSH Manual of Analytical Methods, 2nd ed., V. 4, S120, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 78-175 (1978). Ibid, V. 2, S121, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 77-157-B (1977). Ibid, Vol. 1, P&CAM 253 Criteria for a Recommended Standard . . . Occupational Exposure to Polychlorinated Biphenyls, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 77-225 (1977). Current Intelligence Bulletin 7, Polychlorinated Biphenyls (PCBs), U.S. Department of Health and Human Services, Publ. (NIOSH) 78-127 (1975). Occupational Diseases, A Guide to Their Recognition, revised ed., 255-256, U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 77-181 (1978). Dunker, J. C. and M. T. J. Hillebrand. Characterization of PCB Components in Clophen Formulations by Capillary GC-MS and GC-ECD Techniques, Environ. Sci. Technol., 17 (8), 449456 (1983). Backup Data Report for S120, prepared under NIOSH Contract 210-76-0123, available as "Ten NIOSH Analytical Methods, Set 2," Order No. Pb 271-464 from NTIS, Springfield, VA 22161. NIOSH Research Report-Development and Validation of Methods for Sampling and Analysis of Workplace Toxic Substances, U.S. Department of Health and Human Services, Publ. (NIOSH) 80-133 (1980). Hutzinger, O., S. Safe, and V. Zitko. The Chemistry of PCBs, CRC Press, Inc., Cleveland, OH (1974).
METHOD REVISED BY: James E. Arnold, NIOSH/DPSE; S120 originally validated under NIOSH Contract 210-76-0123.
Table 1. General Information. Compound
CAS
RTECS
Polychlorinated Biphenyls Chlorobiphenyl Aroclor 1016 (41% Cl) Aroclor 1242 (42% Cl) Aroclor 1254 (54% Cl)
1336-36-3 27323-18-8 12674-11-2 53469-21-9 11097-69-1
TQ1350000 DV2063000 TQ1351000 TQ1356000 TQ1360000
NIOSH Manual of Analytical Methods (NMAM), Fourth Edition, 8/15/94
